- 3,4-MDBAL
- 3,4-Methylenedioxybenzaldehyde
- Heliotropin
- Piperonal
Collins, M; Heagney, A; Cordaro, F; Odgers, D; Tarrant, G; Stewart, S. Methyl 3-[3′,4′-(methylenedioxy)phenyl]-2-methyl glycidate: an ecstasy precursor seized in Sydney, Australia. J. Forensic Sci., 1 Jul 2007, 52 (4), 898–903. 714 kB. https://doi.org/10.1111/j.1556-4029.2007.00480.x #Piperonal GC,MS,NMR,IR
Shulgin, AT. Basic Pharmacology and Effects. In Hallucinogens. A Forensic Drug Handbook; Laing, R; Siegel, JA, Eds., Academic Press, London, 24 Apr 2003; pp 67–137. 6.3 MB.
Milhazes, N; Cunha-Oliveira, T; Martins, P; Garrido, J; Oliveira, C; Rego, AC; Borges, F. Synthesis and cytotoxic profile of 3,4-methylenedioxymethamphetamine (“Ecstasy”) and its metabolites on undifferentiated PC12 cells: A putative structure-toxicity relationship. Chem. Res. Toxicol., 1 Oct 2006, 19 (10), 1294–2304. 204 kB. https://doi.org/10.1021/tx060123i #1 MS,NMR,other
Doughty, D; Painter, B; Pigou, P; Johnston, MR. The synthesis and investigation of impurities found in clandestine laboratories: Baeyer-Villiger route part II; Synthesis of phenyl-2-propanone (P2P) analogues from substituted benzaldehydes. Forensic Chem., 1 Jun 2018, 9, 1–11. 2.1 MB. https://doi.org/10.1016/j.forc.2018.03.007 #1g GC,MS,NMR,other
Chambers, SA; DeSousa, JM; Huseman, ED; Townsend, SD. The DARK side of total synthesis: Strategies and tactics in psychoactive drug production. ACS Chem. Neurosci., 17 Oct 2018, 9 (10), 2307–2330. 8.1 MB. https://doi.org/10.1021/acschemneuro.7b00528 #157
Lu, Z; Liang, J; Wang, H; Zhao, S; Zhang, H; Tu, P. Total synthesis of epiberberine. J. Asian Nat. Prod. Res., 1 Sep 2012, 14 (9), 873–876. 74 kB. https://doi.org/10.1080/10286020.2012.701621 #1 MS,NMR
Dunlap, LE; Andrews, AM; Olson, DE. DARK classics in chemical neuroscience: 3,4-Methylenedioxymethamphetamine. ACS Chem. Neurosci., 17 Oct 2018, 9 (10), 2408–2427. 940 kB. https://doi.org/10.1021/acschemneuro.8b00155 #13
Noggle, FT; Clark, CR; Andurkar, S; DeRuiter, J. Methods for the analysis of 1-(3,4-methylenedioxyphenyl)-2-butanamine and N-methyl-(3,4-methylenedioxyphenyl)- 2-propanamine (MDMA). J. Chromatogr. Sci., 1 Mar 1991, 29 (3), 103–106. 760 kB. https://doi.org/10.1093/chromsci/29.3.103 LC,MS,IR
Stein, D. The use of heliotrope oil as a precursor source for piperonal. JCLIC, 1 Jul 1996, 6 (3), 17-18. 575 kB. GC,MS
Plummer, CM; Breadon, TW; Pearson, JR; Jones, OAH. The synthesis and characterisation of MDMA derived from a catalytic oxidation of material isolated from black pepper reveals potential route specific impurities. Sci. Justice, 1 May 2016, 56 (3), 223–230. 630 kB. https://doi.org/10.1016/j.scijus.2016.01.003 #3 GC,NMR
Nair, JB; Hakes, L; Yazar-Klosinski, B; Paisner, K. Fully validated, multi-kilogram cGMP synthesis of MDMA. ACS Omega, 11 Jan 2022, 7 (1), 900–907. 2.6 MB. https://doi.org/10.1021/acsomega.1c05520 #5
White, TJ; Goodman, D; Shulgin, AT; Castagnoli, N; Lee, R; Petrakis, NL. Mutagenic activity of some centrally active aromatic amines in Salmonella typhimurium. Mutat. Res., 1 Jan 1977, 56 (2), 199–202. 256 kB. https://doi.org/10.1016/0027-5107(77)90210-X #3